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Beilstein J. Org. Chem. 2019, 15, 931–936, doi:10.3762/bjoc.15.89
Graphical Abstract
Scheme 1: The reaction of CSI with olefins.
Figure 1: The dipolar intermediate formed in the reaction of CSI with olefins.
Scheme 2: The synthesis of imide 9.
Scheme 3: The synthesis of ylidene sulfamoyl chloride 10.
Figure 2: (a) Molecular structure of racemic molecule 10 (asymmetric unit). Thermal ellipsoids are drawn at t...
Scheme 4: Mechanism for the formation of ylidenesulfamoyl chloride 10.
Figure 3: Relative energy profile of the reaction mechanism shown in Scheme 4.
Beilstein J. Org. Chem. 2010, 6, No. 15, doi:10.3762/bjoc.6.15
Scheme 1: Synthesis of bis-carbamate 12 and oxazolidinone 13.
Scheme 2: Mechanism of the palladium-catalyzed ionization/cyclization reaction.
Scheme 3: Synthesis of aminocyclitol analogue 6.
Figure 1: The thermal ellipsoid plot of the single crystal X-ray crystallographic structure of 18.
Scheme 4: Synthesis of oxazolidone 23.
Scheme 5: Mechanism of the palladium-catalyzed ionization/cyclization reaction in dichloro biscarbamate 22.
Scheme 6: Synthesis of dichloroaminocyclitol 7.
Figure 2: 1H NMR NOE spectrum of compound 7.